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1 article(s) from Manouilidou, Malamatenia D

Staudinger ligation towards cyclodextrin dimers in aqueous/organic media. Synthesis, conformations and guest-encapsulation ability

Malamatenia D. Manouilidou,
Yannis G. Lazarou,
Irene M. Mavridis and
Konstantina Yannakopoulou

Beilstein J. Org. Chem. 2014, 10, 774–783, doi:10.3762/bjoc.10.73

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Scheme 1: (a) Staudinger reaction (b) Staudinger ligation, (c) the cyclodextrin structure with glucopyranose ...

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Scheme 2: (a) i) HCl, NaNO₂/H₂O, then KI/H₂O, 58%, ii) Ph₂PH, Pd(OAc)₂, Et₃N, MeOH, 48%; (b) i) CH₃COOH, H₂SO₄...

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Scheme 3: Staudinger ligation reactions: (a) Preparation of 4 from mono[6-(3-azidopropylamino)-6-deoxy]-β-CD ...

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Figure 1: ¹H NMR chemical shift change (Δδ) of CD cavity Η3 signal of compounds titrated with 1-adamantylamin...

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Figure 2: The most stable conformations of 4 at the PM3(COSMO) level of theory: (a) open, (b) vicinal, and (c...

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Figure 3: Typical conformations of 6: (a) open conformation, (b) vicinal, (c) inclusion/vicinal and (d) doubl...

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Published 03 Apr 2014

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